Analisis Residu Pestisida Sipermetrin Secara GC pada Beras C4 yang Dijual Bebas di Pasar di Kecamatan Ngaglik Kabupaten Sleman Yogyakarta
Abstract
Usage of pesticide which disagree with order, have generated various
problem related to undesirable effect beside that is existence of pesticide reskta.
Considering high enough pesticide toxicity hence needing monitoring of residu
pesticide of sipermetrin in rice which consumed by society in each day. Danger
effect of pesticide of sipermetrin for example: disorder locomotor^ polineuropati,
lmunosupresi, and syndrome of sensitivitas chemical. Government have given
maximal constrain ofpesticide residu which mentioned in " Enclosure Decision Wifll
Minister for Public Health and Minister of Agriculture" No.
881/menkes/SKB/VIII/1996. Sampel taken away from market in region District Of
Ngaglik, that is market of Gentan and market of Rejodani. At this research ofsampel
to be analysed and prepared by counted 100 grams, previous sampel have been
homogenized later; then extracted with acetone/n-heksan. Anumber of extracts
cleaned by chromatography with column of silicagel. Analysis qualitative and
quantitative ofpesticide residu use gas chromatography, equiped by ECD. Obtained
result in the form of retention times and wide area parameter. Rate pesticide of
sipermetrin in rice conducted with wide area of sipermetrin chromatogram in sampel
to equation ofline ofregresi linear ofstandard curve. From research result indicate
that in rice of C4 sold in market in region District of pregnant Ngaglik ofresidu
pesticide of sipermetrin. Mean rate of residu sipermetrin of market of Gentan is 6,07
ppm , while from market of Rejodani is 0,05 ppm. In this research value ofrecovery
mean equal to 95,83 %. From the result can know that rate ofresidu pesticide of
sipermetrin from both market still below/under Maximum Boundary of Residu (
BMR) enabled by Minister for Public Health, that is 5ppm.
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